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1 H NMR (400 MHz, DMSO, 80° C.) δ 8.00 (d, J=8.6 Hz, 1H), 6.46 (s, 1H), 4.54 (d, J=8.7 Hz, 1H), 3.66 (s, 3H), 3.41 (t, J=7.2 Hz, 2H), 3.01 (s, 3H), 2.96 (q, J=7.2 Hz, 2H), 1.92 (s, 3H), 1.70 (quintet, J=7.2 Hz, 2H), 1.40 (s, 9H), 1.31 (s, 3H), 1.30 (s, 3H)

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Then it converts that concentration into a draw volume that matches your research plan